Growth and characterization of di-sodium hydrogen phosphate
Resource
Journal of Crystal Growth 244 (2): 194-199
Journal
Journal of Crystal Growth
Journal Volume
244
Journal Issue
2
Pages
194-199
Date Issued
2002
Date
2002
Author(s)
Gunasekaran, M.
Vijayan, N.
Babu, R. Ramesh
Gopalakrishnan, R.
Ramasamy, P.
Lan, C.W.
DOI
246246/2006111501233470
Abstract
In the present work di-sodium hydrogen phosphate single crystals have been grown from aqueous solution by slow
cooling technique using a constant temperature bath (70.011C). The temperature of the solution was reduced at 0.51C/
day and 0.151C/day from 401C to 351C. Good quality transparent single crystals have been obtained. The solubility of
the material for different temperatures has been studied. The grown crystals were studied by powder and single crystal
X-ray diffraction analyses. The FTIR and UV–visible spectra of the grown crystals were recorded. The thermal
behaviour of the material was studied by simultaneously recorded thermo gravimetric and differential thermal plots.
Subjects
A1. Solubility
A1. Thermal gravimetry
A1. X-ray diffraction
A2. Growth from solutions
B1. Inorganic compounds
Publisher
Taipei:National Taiwan University Dept Chem Engn
Type
journal article
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