Scanning Transmission Electron Microscopy Using Selective High-Order Laue Zones: Three-Dimensional Atomic Ordering in Sodium Cobaltate
Resource
PHYSICAL REVIEW LETTERS, 105(12), 125502
Journal
Physical Review Letters
Pages
125502
Date Issued
2010
Date
2010
Author(s)
Abstract
A new scanning transmission electron microscopy (STEM) imaging technique using high-order Laue zones (named HOLZ-STEM), a diffraction contrast which has been strenuously avoided or minimized in traditional STEM imaging, can be used to obtain the additional 1D periodic information along the electron propagation axis without sacrificing atomic resolution in the lateral (2D) dimension. HOLZ-STEM has been demonstrated to resolve the 3D long-range Na ordering of Na0.71CoO2. Direct evidence of spiral-like Na-trimer chains twisting along the c axis is unambiguously established in real space.
Type
journal article
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