Miceller media accelerated Baylis-Hillman reaction
Resource
CATALYSIS SCIENCE & TECHNOLOGY, 1(9), 1461-1464
Journal
CATALYSIS SCIENCE & TECHNOLOGY
Journal Volume
1
Journal Issue
9
Pages
1461-1464
Date Issued
2011
Date
2011
Author(s)
Pawar, Balu
Padalkar, Vikas
Phatangare, Kiran
Nirmalkar, Sudhakar
Chaskar, Atul
Abstract
Triton X-100 aqueous micelle accelerates the rate of Baylis–Hillman reaction and enhances the product yield. The type and concentration of surfactants play prominent roles in the reaction. An aqueous micelle Triton X-100 is easily recovered and reused for four runs without substantial loss in yield. 1,4-diazabicyclo[2.2.2]octane (DABCO) (20 mol%) is found to be a good basic catalyst in aqueous micelle. Apparently, this protocol has several advantages such as green reaction medium, mild reaction condition, ease of product recovery and moderate-to-good yield of product.
Type
journal article
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