Microwave-Assisted Cross-Coupling for the Construction of Diaryl Sulfides
Resource
JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 58(1), 94-100
Journal
JOURNAL OF THE CHINESE CHEMICAL SOCIETY
Journal Volume
58
Journal Issue
1
Pages
94-100
Date Issued
2011
Date
2011
Author(s)
Abstract
Abstract The construction of diaryl sulfides through the cross‐coupling of aryl iodides and thiols in microwave heating is described. By using this method, a variety of diaryl sulfides can be prepared in a mild condition and in high yields. Deactivated 4‐nitrothiophenol was effective to afford the product in 94% yield. Sterically hindered ortho ‐substituted aryl iodides or thiophenols provided diaryl sulfides effectively by this microwave‐assisted coupling reaction.
Type
journal article
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